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Distortion of the Trigonal-Bipyramidal Ligand Arrangement in Bicyclophosphoranes—Structure of 2,3,8,8- Tetraphenyl[1,3,2λ5]oxazaphospholino[2,3-b]benzo[d]-[1,3,2λ5]oxazaphospholine

✍ Scribed by Dr. William S. Sheldrick; Priv.-Doz. Dr. Alfred Schmidpeter; Josef Helmut Weinmaier


Publisher
John Wiley and Sons
Year
1975
Tongue
English
Weight
232 KB
Volume
14
Category
Article
ISSN
0044-8249

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K 2 W 6 Br 14 (I), Rb 2 W 6 Br 14 (II), and Cs 2 W 6 Br 14 (III) were formed by reactions of W 6 Br 12 with the corresponding alkali metal bromides in evacuated silica tubes with a temperature gradient of 925 K/915 K. (I) crystallizes in the cubic space group Pn3 (no. 201), a = 13.808 A Ê , Z = 4, c