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Direkte Beobachtung des Zentralatoms in [C{Au[P(C6H5)2(p-C6H4NMe2)]}6](BF4)2 durch 13C-NMR-Spektroskopie

✍ Scribed by Prof. Dr. Hubert Schmidbaur; Benno Brachthäuser; Oliver Steigelmann

Publisher
John Wiley and Sons
Year
1991
Tongue
English
Weight
259 KB
Volume
103
Category
Article
ISSN
0044-8249

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Reaction of elemental antimony with sulfur under mild hydrothermal conditions yielded different polysulfidoclusters of antimony. These were isolated as tetraphenylphosphonium salts [P(C 6 H 5 ) 4 ] 3 Sb 3 S 25 and [P(C 6 H 5 ) 4 ] 2 Sb 2 S 15 2(C 3 N 2 H 6 ) and their crystal structures were determi