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Direct Synthesis of β-Aminoketones from Amides via Novel Sequential Nucleophilic Substitution/Michael Reaction †

✍ Scribed by Gomtsyan, Arthur

Book ID: 126429172
Publisher: American Chemical Society
Year: 2000
Tongue: English
Weight: 113 KB
Volume: 2
Category: Article
ISSN: 1523-7060
DOI: 10.1021/ol9911122

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## Abstract magnified image 3‐Imino‐2‐amino‐isatines were obtained by a one‐pot reaction of an excess of aniline (or its derivatives) with 1,2‐bis(dimethylamino)‐1,2‐dichloro‐ethene (prepared __in situ__ from DMF). Subsequent hydrolysis yielded the corresponding isatine derivatives in reasonable t