## Liquid chromatographic direct resolution of b-amino acids on a chiral crown ether stationary phase A chiral stationary phase (CSP) prepared by bonding (+)-(18-crown-6)-2,3,11,12tetracarboxylic acid to silica gel was used for the direct resolution of b-amino acids. To determine the optimum mobil
✦ LIBER ✦
Direct separation of amino acid enantiomers using a chiral crown ether stationary phase: Application to 2-amino-ω-phosphonoalkanoic acids
✍ Scribed by Peter M. Udvarhelyi; David C. Sunter; J.C. Watkins
- Publisher
- Elsevier Science
- Year
- 1990
- Tongue
- English
- Weight
- 351 KB
- Volume
- 519
- Category
- Article
- ISSN
- 1873-3778
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## Abstract A chiral stationary phase (CSP **1**) based on (+)‐(18‐crown‐6)‐2,3,11,12‐tetracarboxylic acid was applied to the resolution of __N__‐(substituted benzoyl)‐α‐amino acid amides and esters. __N__‐(Substituted benzoyl)‐α‐amino acid amides were well resolved using a mixture of acetic acid‐t