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Direct observation of radical intermediates in the photo-Kolbe reaction - heterogeneous photocatalytic radical formation by electron spin resonance

โœ Scribed by Kraeutler, Bernhard; Jaeger, Calvin D.; Bard, Allen J.


Book ID
118252970
Publisher
American Chemical Society
Year
1978
Tongue
English
Weight
439 KB
Volume
100
Category
Article
ISSN
0002-7863

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Direct observation of the unstable inter
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## Abstract Direct observation of the unstable intermediate in the radical addition reaction of the oxime ether 1 mediated by triethylborane (Et~3~B) is described using ^1^H and ^11^B micro channeled cell for synthesis monitoring (MICCS), which was recently developed as an interfacing microchip for