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Direct observation of (H8,H6)-Hr J-coupling correlations in oligonucleotides for unambiguous resonance assignments: Use of J-scaling in two-dimensional correlated spectroscopy

โœ Scribed by Praful Gundhi; K.V.R. Chary; R.V. Hosur


Book ID
115917276
Publisher
Elsevier Science
Year
1985
Tongue
English
Weight
466 KB
Volume
191
Category
Article
ISSN
0014-5793

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Assignment of resonances in the 1H spect
โœ Kevin L. Behar; Takashi Ogino ๐Ÿ“‚ Article ๐Ÿ“… 1991 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 1011 KB

Two-dimensional shift-correlated (COSY) and J-resolved NMR spectroscopy was used to identify and assign resonance in the aliphatic region (0.8 to 4.5 ppm) of the 1H spectrum of acid extracts and tissue of rat brain. The chemical shift and spin-spin coupling constants of several resonances, which cou