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Direct Observation of Carbene and Diazo Formation from Aryldiazirines by Ultrafast Infrared Spectroscopy

✍ Scribed by Zhang, Yunlong; Burdzinski, Gotard; Kubicki, Jacek; Platz, Matthew S.

Book ID: 126886705
Publisher: American Chemical Society
Year: 2008
Tongue: English
Weight: 542 KB
Volume: 130
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja805922b

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The [2 + 1] cycloaddition reaction of electron-rich alkenes such as enol ethers with 9-diazo-9H-fluorene (1) is efficiently catalyzed by pentacarbonyl(η 2 -cis-cyclooctene)chromium(0) (2). This cyclopropanation reaction shows a pronounced preference for electron-rich C=C bonds, as demonstrated by th