Direct Evidence for Oxygen-Atom Exchange
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Mi Sook Seo; Jun-Hee In; Sun Ok Kim; Na Young Oh; Jongki Hong; Jinheung Kim; Law
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Article
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2004
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John Wiley and Sons
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English
โ 139 KB
Complexes 1 and 2 were prepared by treating [Fe(TMC)(OTf) 2 ] (2 mm) and [Fe(N4Py)(ClO 4 ) 2 ] (2 mm), respectively, with 1 equivalent of peracid (peracetic acid for 1 and m-chloroperbenzoic acid for 2) in CH 3 CN (3 mL) at 10 8C. [7] After appropriate amounts of H 2 18 O were added to the reaction