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Direct Evidence for a Nitrile Imine–Imidoylnitrene Rearrangement: X-Ray Crystal Structure of an Unusual Nitrene Complex

✍ Scribed by Michel Granier; Dr. Antoine Baceiredo; Dr. Hansjörg Grüzmacher; Dr. Hans Pritzkow; Dr. Guy Bertrand


Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
340 KB
Volume
29
Category
Article
ISSN
0044-8249

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✦ Synopsis


In this case photobromindtion was carried out in the presence of small amounts of AcONa to neutralize HBr developed during the reaction, becduse. under irradiation. HBr promoted a fast protodesilylation of the starting benzyltrimethylsilane. Addition of AcONa had no effect on the product composition of the photobromination of 1 in AcOH.

[6] P.