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Direct determination of leucine metabolism and protein breakdown in humans using L-[1-13C, 15N]-leucine and the forearm model

โœ Scribed by K. N. CHENG; F. DWORZAK; G. C. FORD; M. J. RENNIE; D. HALLIDAY

Book ID
114726494
Publisher
John Wiley and Sons
Year
1985
Tongue
English
Weight
489 KB
Volume
15
Category
Article
ISSN
0014-2972

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Stereoselective synthesis of stable isot
Stereoselective synthesis of stable isotope-labeled L-ฮฑ-amino acids: Electrophilic amination of Oppolzer's acyl sultams in the synthesis of L-[15N]alanine, L-[15N]valine, L-[15N]leucine, L-[15N]phenylalanine and L-[1-13C, 15N]valine
โœ Siegfried N. Lodwig; Clifford J. Unkefer ๐Ÿ“‚ Article ๐Ÿ“… 1996 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 475 KB ๐Ÿ‘ 1 views

Using 1 -chloro-l-[~~N]nitrosocyclohexane, we have prepared five L-[a-'SN]arnino acids. The stereoselective electophillic hydroxyamination of (S)-acylbornane-l0,2-suftams, followed by ZnO/H+ reduction, and alkaline cleavage of the chiral auxiliary, gave the amino acids in 97.2-99.5 % e.e. By starti