Dipolar local field measurements from indirect observation of 1H nuclei via cross-polarization 13C nuclear magnetic resonance spectroscopy

✍ Scribed by P. Palmas; P. Tekely; D. Canet

• Book ID: 103963722
• Publisher: Elsevier Science
• Year: 1995
• Tongue: English
• Weight: 585 KB
• Volume: 4
• Category: Article
• ISSN: 0926-2040
• DOI: 10.1016/0926-2040(94)00037-d

✦ Synopsis

An extension

of the exploitation of a simple pulse sequence designed for indirect observation of 'H nuclei through 13C resonances is presented.

It is shown that by using this pulse sequence under conditions of rapid magic-angle rotation and coherent energy transfer between directly bonded protons and carbons, an insight into the local dipolar interactions is available in typical organic solids.

* Dedicated to Prof. J.J. Delpuech on the occasion of his 60th birthday, presented in part at the 12th European Experimental NMR Conference,