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Dinuclear 2,2′-biallyl nickel complexes containing square-planar nickel(I): crystal structure of μ(η3;3-(CH2)2CC(CH2)2)-trans- [Ni(dad)]2 (dad = biacetylbis(2,6-dimethylphenylimine))

✍ Scribed by J. Sinnema; H. tom Dieck; G. Fendesak

Publisher: Elsevier Science
Year: 1990
Tongue: English
Weight: 450 KB
Volume: 397
Category: Article
ISSN: 0022-328X
DOI: 10.1016/0022-328x(90)80245-u

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## Abstract The preparation of a family of dinuclear monocyclopentadienyl imidoniobium and ‐tantalum complexes was achieved by two different synthetic routes. The diimido complexes [{M(Cp′)Cl~2~}~2~(μ‐1,__i__‐NC~6~H~4~N)] [Cp′ = η^5^‐C~5~H~4~SiMe~3~, M = Nb, __i__ = 4 (1); Cp′ = η^5^‐C~5~H~4~SiMe~3