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Dimers from cyclic α-diketones. Confirmation of structure by solid-phase CPMAS 13C NMR spectroscopy

✍ Scribed by Roger S. Macomber; Paul Murphy


Publisher
John Wiley and Sons
Year
1984
Tongue
English
Weight
183 KB
Volume
22
Category
Article
ISSN
0749-1581

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✦ Synopsis


The solid-phase "C CPMAS NMR spectra of the crystallime h e r s from lo-, 12and 14-membered cyclic a-diketones were found to be in full accord with the symmeirical tricyclic 2,5-dihydroxycyclohexane-l,4dione structures previously proposed on the basis of molecular formulae and in€rared spectroscopy.