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Diiron Azadithiolates as Models for the Iron-Only Hydrogenase Active Site: Synthesis, Structure, and Stereoelectronics

✍ Scribed by Joshua D. Lawrence; Hongxiang Li; Thomas B. Rauchfuss; Marc Bénard; Marie-Madeleine Rohmer

Publisher: John Wiley and Sons
Year: 2001
Tongue: English
Weight: 110 KB
Volume: 113
Category: Article
ISSN: 0044-8249
DOI: 10.1002/1521-3757(20010504)113:9<1818::aid-ange18180>3.0.co;2-h

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## Abstract We have developed a simple and convenient method for the synthesis of the first H‐cluster models in which a L‐cysteinyl group is coordinated to one of the two iron atoms of the diiron subsite through its sulfur atom. This synthetic method includes (i) treatment of the Boc‐protected L‐cy