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Diethylsilyl ether and diethylsiliconide derivatives in gas chromatography mass spectrometry of hydroxylated steroids

✍ Scribed by Hiroshi Miyazaki; Masataka Ishibashi; Masahiro Itoh; Kouwa Yamashita

Publisher
John Wiley and Sons
Year
1984
Tongue
English
Weight
489 KB
Volume
11
Category
Article
ISSN
1076-5174

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Allyldimethylsilyl ethers of prostaglandin E2 and F, , leukotriene B4 and S@-pregnane3a, 2Oa-diol were prepared at room temperature in good yields with the novel reagent N,O-bis(allyldimethyIsi1yl)-trifluoroacetamide. The gas chromatographic properties of the derivatives of prostaglandins and the st