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Diethoxyphosphinylethylidene acetals of d-mannitol and d-glucitol

✍ Scribed by Shaul Yanai; Mordehai Halmann; David Vofsi

Book ID
108308561
Publisher
Elsevier Science
Year
1980
Tongue
English
Weight
273 KB
Volume
83
Category
Article
ISSN
0008-6215

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Ethylidenation of 1,6-di-O-benzoyl-2,4-0-benzylidene-o-glucitol gave the 3,5-0-ethylidene derivative in poor yield, whereas reaction with 2,2\_dimethoxypropane gave the 3,5-0-isopropylidene derivative in good yield. Removal of the benzoyl and benzylidene groups, with further derivatisation, gave a v