In a recent communication'). we reported the synthesis of some biologically interesting 1-substituted 3-(2-perimidyl)-ureas starting from 2-aminoperimidine (la). Because of the presence of a 1,3-dinucleophilic center in this molecule, l a might undergo cyclocondensation with appropriate dielectrophi
✦ LIBER ✦
Die Kristallstruktur von 1,2,3,4-Tetrahydro-1-methyl-2-oxopyrimido[1,2-a]benzimidazol-4-carbonsäuremethylester
✍ Scribed by Hans Peter Weber; Franz Troxler
- Publisher
- John Wiley and Sons
- Year
- 1974
- Tongue
- German
- Weight
- 283 KB
- Volume
- 57
- Category
- Article
- ISSN
- 0018-019X
No coin nor oath required. For personal study only.
✦ Synopsis
The crystal structure of 1,2,3,4‐Tetrahydro‐1‐methyl‐2‐oxopyrimido[1,2‐a]benzimidazol‐4‐carboxylicacid‐methylester was investigated by an X‐ray analysis in order to determine unequivocally the positions of the substituents. The triclinic structure was solved by the multisolution method and refined to an R = 0.0302 with 1486 structure factors for 222 structural parameters.
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