Coordination Chemistry of Polyoxomolybda
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Qin Chen; Shuncheng Liu; Professor Jon Zubieta
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Article
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1990
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John Wiley and Sons
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English
⚖ 387 KB
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I : A suspension of 1 g of TiCI, in 15 mL of dry CH,CN was heated under reflux in an inert atmosphere (Ar) until a deep-blue solution was obtained. This was then treated dropwise with a solution of 1.2 g of N,N',N"-trimethyl-l,4,7-triazacyclononane (L) in 10 mL of CH,CN. After 30 minutes' stirring a