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Die Koordinationschemie von Polyoxomolybdaten: Die Struktur eines zwölfkernigen Molybdat-Käfigs mit Hydrogenquadratat-Liganden, [(C4H9)4N]4[Mo12O36(C4O4H)4] · 10(C2H5)2O

✍ Scribed by Qin Chen; Shuncheng Liu; Prof. Jon Zubieta


Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
330 KB
Volume
102
Category
Article
ISSN
0044-8249

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Coordination Chemistry of Polyoxomolybda
✍ Qin Chen; Shuncheng Liu; Professor Jon Zubieta 📂 Article 📅 1990 🏛 John Wiley and Sons 🌐 English ⚖ 387 KB 👁 1 views

I : A suspension of 1 g of TiCI, in 15 mL of dry CH,CN was heated under reflux in an inert atmosphere (Ar) until a deep-blue solution was obtained. This was then treated dropwise with a solution of 1.2 g of N,N',N"-trimethyl-l,4,7-triazacyclononane (L) in 10 mL of CH,CN. After 30 minutes' stirring a