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Diastereoselective Vinyl Phosphate/β-Keto Phosphonate Rearrangements

✍ Scribed by An, Jianguo; Wilson, Jeffrey M.; An, Yi-Zhong; Wiemer, David F.

Book ID
121498691
Publisher
American Chemical Society
Year
1996
Tongue
English
Weight
256 KB
Volume
61
Category
Article
ISSN
0022-3263

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Diastereoselective synthesis of β-amino-
Diastereoselective synthesis of β-amino-α-hydroxy phosphonates via oxazaborolidine catalyzed reduction of β-phthalimido-α-keto phosphonates
✍ Achille Barco; Simonetta Benetti; Paola Bergamini; Carmela De Risi; Paolo Marche 📂 Article 📅 1999 🏛 Elsevier Science 🌐 French ⚖ 221 KB

Reduction of I~-phthalimido-et-keto phosphonates, obtained through an Arbuzov reaction between the appropriate acid chloride and triethyl phosphite, with boranes and oxazaborolidine as catalyst, afforded I~-phthalimido-0t-hydroxy phosphonates in good yields and high diastereoselectivity. Deprotectio