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Diastereoselective Formation of Cyanohydrins from α-Alkoxy Aldehydes

✍ Scribed by Ward, Dale E.; Hrapchak, Matthew J.; Sales, Marcelo

Book ID
120460691
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
53 KB
Volume
2
Category
Article
ISSN
1523-7060

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Lewis acid promoted aldol additions of α
Lewis acid promoted aldol additions of α-thiosilylketeneacetals to α-alkoxy aldehydes: diastereoselective synthesis of syn-α-methylene-β-hydroxy-∂-alkoxy esters.
✍ Anna Bernardi; Silvia Cardani; Cesare Gennari; Giovanni Poli; Carlo Scolastico 📂 Article 📅 1985 🏛 Elsevier Science 🌐 French ⚖ 190 KB

MgBr mediated addition of to A'and Methyl &-methylthio propionate silylketene acetal o(,p-alkoxy aldehydes is highly 3,4 syn-selective (18:l). syn-d-methylene$-hydroxy-s-alkoxy esters (6) and (8) are synthesized. We recently reported that I butyIP-dimethylamino propionate, a synthetic equivalent of