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Diastereoselective desulfurization of 5,6-dihydro-1,4-dithiins. Synthesis of muscalure from Musca domestica L.

✍ Scribed by Romualdo Caputo; Giovanni Palumbo; Silvana Pedatella

Publisher
Elsevier Science
Year
1994
Tongue
French
Weight
345 KB
Volume
50
Category
Article
ISSN
0040-4020

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✦ Synopsis

Abstmct: A procedure is reported for the chemo-and stereo-selective sulfur removal from 5,6-dihydm-1,4-dithiins which completes the pathway to synthesize cis configurated olefms from carbonyl compounds. A four step synthesis of (Z)-9-tricosene (muscalure) with the dithiin moiety serving as the penultimate olefm precursor is also reported as an example of the proposed syntbelic strategy.

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