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Di-μ-hydroxido-bis[aquatrichloridotin(IV)] benzene hemisolvate monohydrate

✍ Scribed by Müller, Manuela ;Lerner, Hans-Wolfram ;Bolte, Michael

Publisher: International Union of Crystallography
Year: 2007
Tongue: English
Weight: 352 KB
Volume: 63
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536807049185

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✦ Synopsis

In the title compound, [Sn~2~Cl~6~(OH)~2~(H~2~O)~2~]·0.5C~6~H~6~·H~2~O, the benzene molecule is located on a centre of inversion. The Sn atoms are in an octahedral environment, each coordinated by three Cl, one water and two briding hydroxide ligands. Two Cl atoms and the hydroxide groups are in the equatorial plane, whereas the third Cl atom and the water molecules are located in the axial positions.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.015 A Ê Disorder in solvent or counterion R factor = 0.038 wR factor = 0.109 Data-to-parameter ratio = 13.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.