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Development of new linkers for the formation of aliphatic C-H bonds on polymeric supports

✍ Scribed by Kyung Woon Jung; Xy-yang Zhao; Kim D. Janda

Book ID: 104207729
Publisher: Elsevier Science
Year: 1997
Tongue: French
Weight: 532 KB
Volume: 53
Category: Article
ISSN: 0040-4020
DOI: 10.1016/s0040-4020(97)00222-6

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✦ Synopsis

Two polymeric linkers, 8 and II, were prepared in high yields. Aftachment of an alkyl group to these linkers was facile, and their cleavage from the MeO-PEG polymer support was accomplished by desulfurization using Raney nickel to yield the new carbon-hydrogen bond product 6. The protocol reported herein allows ejjicient preparation of new polymeric linkers as well as their possible application to combinatorial libraries. 0 1997

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