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Deuterium quadrupole echo NMR spectroscopy II. Artifact suppression

✍ Scribed by Alan D Ronemus; Robert L Vold; Regitze R Vold


Publisher
Elsevier Science
Year
1986
Weight
885 KB
Volume
70
Category
Article
ISSN
0022-2364

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2D spectra, particularly for homonuclear correlation, can show a variety of artifactual signals in the F 1 domain. Common sources include carry-over of signal modulation from one transient to the next ("rapid pulsing artifacts") and systematic variations in room temperature ("parallel diagonals"). I