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Deuterium quadrupole couplings from least-squares computer simulations of 2H MAS NMR spectra

✍ Scribed by Jørgen H Kristensen; Henrik Bildwe; Hans J Jakobsen; Niels Chr Nielsen


Publisher
Elsevier Science
Year
1991
Weight
634 KB
Volume
92
Category
Article
ISSN
0022-2364

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Computer simulations of 2H MAS NMR spinn
✍ N.J. Clayden 📂 Article 📅 1986 🏛 Elsevier Science 🌐 English ⚖ 486 KB

The quadrupole coupling constant and asymmetry parameter of a \*H MAS NMR spectrum can be derived by computer simulations of the spinning sideband pattern. Off angle spinning causes complex lineshapes which can be used to find approximate quadrupole parameters and to determine more accurately the as