𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Determination of vinyl acetate in air by gas chromatography

✍ Scribed by Kirpal S. Sidhu

Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
315 KB
Volume
1
Category
Article
ISSN
0260-437X

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

A gas chromatographic analysis for vinyl acetate is presented. Vinyl acetate was sampled by adsorbing on activated carbon. It was desorbed with carbon disulfide with a mean efficiency of 83.0%. The analytical column was packed with 10% free fatty acid phase on acid‐washed Chromosorb‐P. Gas chromatographic identification was also conducted on another column packed with 0.4% Carbowax‐1500 on Carbopack A. Analysis was performed on a chromatograph equipped with a flame ionization detector. The precision (coefficient of variation) for the analytical procedure using a free fatty acid phase column was 4.0%. Based on a 10 litre air sample, the calculated limit of detection by this procedure was 0.1 parts per million.

πŸ“œ SIMILAR VOLUMES

Determination of adsorption by fluoresce
Determination of adsorption by fluorescence in gas chromatography
✍ Driessen, O. ;Lugtenberg, J. πŸ“‚ Article πŸ“… 1980 πŸ› John Wiley and Sons 🌐 English βš– 439 KB πŸ‘ 1 views

## Abstract PMBF~2~, a pyrromethene pigment, can be used in gas chromatography. Because of its fluorescence, adsorption sites on glass columns and connections can be traced in situ. The compound can be employed to check the inertness of glass surfaces after deactivation procedures. Some application

Determination of chlorobutanol in pharma
Determination of chlorobutanol in pharmaceuticals by gas chromatography
✍ K. T. Koshy; R. C. Conwell; R. N. Duvall πŸ“‚ Article πŸ“… 1967 πŸ› John Wiley and Sons 🌐 English βš– 305 KB

A gas chromatographic procedure has been developed for the determination of chlorobutanol in a variety of pharmaceutical preparations. Numerous columns were investigated and found useful. Chlorobutanol was separated from its degradation products o n all of these columns. Analysis of synthetic mixtur