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Determination of urinary tetrahydrocortisone tetrahydrocortisol and 3α-allotetrahydrocortisol by gas chromatography

✍ Scribed by M. Sparagana

Book ID
118977144
Publisher
Elsevier Science
Year
1965
Tongue
English
Weight
824 KB
Volume
6
Category
Article
ISSN
0039-128X

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✍ H. Wieczorek; B. Trojanowska; W. Dramiński 📂 Article 📅 1979 🏛 Springer-Verlag 🌐 English ⚖ 476 KB

The determination of benzoic, 3- and 4-methylbenzoic, and mandelic acids in urine by gas chromatography (G.C.) is presented. The analytical procedure includes: addition of internal standard (beta-naphthol), alkaline hydrolysis, ethyl ether extraction, evaporation of the solvent, and silylation of ac