cis-1,3,6,8,10b,10c-Hexamethyl-10b,10c-d
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GrahamΒ J. Bodwell; JohnΒ N. Bridson; Shu-Ling Chen; Jiang Li
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Article
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2002
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John Wiley and Sons
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English
β 297 KB
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The title compound was prepared as part of an effort to accomplish the first synthesis of a cis-10b,10c-dimethyl-10b,10c-dihydropyrene according to our ''tethered metacyclophane'' strategy. The 11-step synthesis starting from 2,4,6trimethylphenol had an overall yield of 4.1%. An X-ray crys- The 10b