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Determination of the enantiomerization barrier of thalidomide by dynamic capillary electrokinetic chromatography

✍ Scribed by Gabriele Schoetz; Oliver Trapp; Volker Schurig


Publisher
John Wiley and Sons
Year
2001
Tongue
English
Weight
80 KB
Volume
22
Category
Article
ISSN
0173-0835

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A micellar electrokinetic capillary chromatographic method was set up for the separation of five anthraquinone derivatives in rhubarb. Optimization of pH and sodium deoxycholate(SDC) concentrations was studied, which showed that 50 mM H3BO3-NaOH(pH 11) containing 25 mM SDC could separate the five in