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Determination of the conformation of 1,4-diheterocyclanes. I—The 1H n.m.r. spectrum and ring conformation of 3-methyl-2-oxo-1,4-dioxepane

✍ Scribed by Pertti Äyräs; Annikki Partanen


Publisher
John Wiley and Sons
Year
1977
Tongue
English
Weight
245 KB
Volume
9
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

The ^1^H n.m.r. spectrum of 3‐methyl‐2‐oxo‐1,4‐dioxepane was recorded at 300 and 60 MHz. The ring conformation was considered in terms of the spectral parameters and shown to be a twisted boat where the lactone grouping is approximately planar.


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