Determination of the chirality of amino acid residues in the course of subtractive edman degradation of peptides
β Scribed by Andrea Scaloni; Maurizio Simmaco; Francesco Bossa
- Book ID
- 107718967
- Publisher
- Elsevier Science
- Year
- 1991
- Tongue
- English
- Weight
- 571 KB
- Volume
- 197
- Category
- Article
- ISSN
- 0003-2697
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π SIMILAR VOLUMES
DABS-Cl, dimethylaminoazobenzenesulfonyl chloride; DABITC, dimethylaminoazobenzene isothiocyanate; DABTC, dimethylaminoazobenzene thiocarbamyl; PTH, phenylthiohydantoin. ' Results were averaged from two separate analysis of approx 15-20 ng of dabsylated eglin c hydrolysate.
The stereochemistry of both the N,N-dimethyl amino acid and a-amino acid residues, after hydrolysis of the peptide alkaloids scutianine-B, -C, -D and -E, franganine and adoutine-Y' have been determined by gas chromatography employing modified cyclodextrins as chiral stationary phases.