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Determination of sulphate isotopomers by vibrational spectroscopy

✍ Scribed by Brian J. Reedy; James K. Beattie; Richard T. Lowson

Publisher: Elsevier Science
Year: 1990
Tongue: English
Weight: 551 KB
Volume: 46
Category: Article
ISSN: 1386-1425
DOI: 10.1016/0584-8539(90)80065-7

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On reaction with N,N-dichloro-t-butylamine or -cyclohexylamine in benzene at 0 "C, nickel tetracarbonyl evolves three moles of carbon monoxide per mole. A colorless precipitate ( I ) is formed that has a Ni:N ratio of 1 : 1 and is insoluble in the usual solvents. 2 RNClz + 2 Ni(CO)4 + 2 [RNClzNi(CO)