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Determination of soil amino acids by high performance liquid chromatography-electro spray ionization-mass spectrometry derivatized with 6-aminoquinolyl-N-hydroxysuccinimidyl carbamate

โœ Scribed by Songmei Hou; Hongbo He; Wei Zhang; Hongtu Xie; Xudong Zhang


Book ID
116903902
Publisher
Elsevier Science
Year
2009
Tongue
English
Weight
667 KB
Volume
80
Category
Article
ISSN
0039-9140

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A highly reactive amine derivatizing reagent, 6-aminoquinolyl-N-hydroxysuccinimidyl carbamate, has been synthesized. In a rapid, one-step procedure, the compound reacts with amino acids to form stable unsymmetric urea derivatives which are readily amenable to analysis by reversed phase HPLC. Studies