Determination of oxygen/metal ratios for uranium, plutonium, and (U, Pu) mixed oxides
β Scribed by C.E. McNeilly; T.D. Chikalla
- Publisher
- Elsevier Science
- Year
- 1971
- Tongue
- English
- Weight
- 661 KB
- Volume
- 39
- Category
- Article
- ISSN
- 0022-3115
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π SIMILAR VOLUMES
A known amount of lithium or calcium nitrate solution is added to the sample powder which is then heated in air or oxygen. The oxygen in test samples of UO,+,, SrO.,UO.,O,+, and SrO.,UO.,O,+, was determined with an estimated standard deviation of +\_ 0.002.
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Over the temperature range \(150-550^{\circ} \mathrm{C}\), the temperatures of oxidation peaks of transition metal ions in submicrometer-sized ferrites with the spinel structure, obtained by DTG, have been related to their cation-oxygen distances. A data table comparing oxidation temperature and cat