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Determination of organometallic compounds by capillar gas chromatography - inductively coupled plasma mass spectrometry

✍ Scribed by Kim, Alexander ;Hill, Steve ;Ebdon, Les ;Rowland, Steve

Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
305 KB
Volume
15
Category
Article
ISSN
0935-6304

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✦ Synopsis

Abstract

The separation and detection of volatile organometallic compounds containing tin, iron, and nickel has been achieved using capillary GC–inductively coupled plasma–mass spectrometry (capillary GC‐ICP‐MS). Detection limits range from 3.0 to 7.0 pg/s. The presence of volatile organotin compounds in a harbor sediment has been confirmed. The retention range of the organometallic compounds analyzed by capillary GC‐ICP‐MS has been extended considerably beyond that possible in earlier studies (retention indices up to 3400).

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