𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Determination of organochlorine pesticide residues by solid phase extraction and dual-column HRGC

✍ Scribed by Torreti, Luigi ;Simonelia, Anselmo ;Dossena, Angelo ;Torreti, Emilio

Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
300 KB
Volume
15
Category
Article
ISSN
0935-6304

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

Organochlorine pesticide residues have been extracted from samples of animal feed by a solid phase extraction clean‐up procedure using an octadecyl‐bonded column. The proposed method gave recoveries ranging from 70 to 100 % for ppb levels of the fifteeen pesticides studied. Analytes were identified by dual‐column capillary gas chromatography employing DB‐1 and DB‐1701 columns in parallel; identities were confirmed by calculation of retention indexes with the cubic spline interpolation method.

📜 SIMILAR VOLUMES

Evaluation of a solid phase extraction p
Evaluation of a solid phase extraction procedure for the determination of pesticide residues in foodstuffs
✍ Barwick, Vicki J; Ellison, Stephen L?R; Lacey, Sharon J; Mussell, Chris R; Lucki 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 89 KB 👁 2 views

An evaluation of a method based on solid phase extraction (SPE) as a clean-up stage for the determination of pesticide residues in composite vegetable and cabbage samples is presented. Samples are extracted with acetonitrile and the extract is loaded onto an SPE cartridge. The pesticides are eluted

Multi-residue determination of organopho
Multi-residue determination of organophosphorus and organochlorine pesticides in environmental samples using solid-phase extraction with cigarette filter followed by gas chromatography–mass spectrometry
✍ Guozhen Fang; Wen Chen; Yunping Yao; Junping Wang; Junyan Qin; Shuo Wang 📂 Article 📅 2012 🏛 John Wiley and Sons 🌐 English ⚖ 134 KB

## Abstract A solid‐phase extraction (SPE) method was developed to extract 14 pesticides simultaneously from environment samples using cigarette filter as the sorbent before gas chromatography‐mass spectrometry (GC‐MS) analysis. Parameters influencing the extraction efficiency, such as the sample l

Extraction and Clean-Up Method for the D
Extraction and Clean-Up Method for the Determination of Twenty Organochlorine Pesticide Residues in Tomatoes by GLC-ECD
✍ Morelli-Cardoso, Maria Helena W. ;Cardozo, Regina T. M. ;Mello, Jaíza L. ;Abrant 📂 Article 📅 1999 🏛 John Wiley and Sons 🌐 English ⚖ 48 KB 👁 2 views

A method is described for the simultaneous extraction and determination of twenty organochlorine pesticides residues [hexachlorocyclohexane (HCH) isomers (a, b, c, d), aldrin, dieldrin, endrin, heptachlor and its epoxide (HE), hexachlorobenzene (HCB), a-endosulfan, o,p9-DDD, p,p9-DDD, o,p9-DDE, p,p9

Solid-phase extraction and residue deter
Solid-phase extraction and residue determination of glyphosate in apple by ion-pairing reverse-phase liquid chromatography with pre-column derivatization
✍ Kun Qian; Tao Tang; Tianyu Shi; Pingliang Li; Jianqiang Li; Yongsong Cao 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 English ⚖ 372 KB 👁 1 views

## Abstract A new method for glyphosate residue determination in apple has been developed. A SPE cartridge was used to clean up the samples before derivatization. Glyphosate was derivatized with 4‐chloro‐3,5‐dinitrobenzotrifluoride (CNBF) and quantified by reverse ion‐pair liquid chromatography usi