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Determination of Mercury in Urine

✍ Scribed by Miller, V. L.; Swanberg, Frank.

Book ID
127342209
Publisher
American Chemical Society
Year
1957
Tongue
English
Weight
398 KB
Volume
29
Category
Article
ISSN
0003-2700

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A simple, rapid and accurate method was developed for the determination of total mercury in urine samples . The method uses on-line addition of KMnO4 after adding a bromate-bromide reagent to the sample to decompose organic mercury compounds to inorganic mercury(II) ions at room temperature, and det

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Differential pulse stripping voltammetry was applied in the determination of mercury in urine samples. The mercury in the samples was oxidized to Hg(II) using bromine and KMnO 4 . Hg(II) was reduced by NaBH 4 to the metallic state and volatilized using nitrogen as the carrier gas. The gas containing