𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Determination of matrix composition based on solute-solute nearest-neighbor distances in atom probe tomography

✍ Scribed by F. De Geuser; W. Lefebvre


Publisher
John Wiley and Sons
Year
2011
Tongue
English
Weight
377 KB
Volume
74
Category
Article
ISSN
1059-910X

No coin nor oath required. For personal study only.

✦ Synopsis


Abstract

In this study, we propose a fast automatic method providing the matrix concentration in an atom probe tomography (APT) data set containing two phases or more. The principle of this method relies on the calculation of the relative amount of isolated solute atoms (i.e., not surrounded by a similar solute atom) as a function of a distance d in the APT reconstruction. Simulated data sets have been generated to test the robustness of this new tool and demonstrate that rapid and reproducible results can be obtained without the need of any user input parameter. The method has then been successfully applied to a ternary Al‐Zn‐Mg alloy containing a fine dispersion of hardening precipitates. The relevance of this method for direct estimation of matrix concentration is discussed and compared with the existing methodologies. Microsc. Res. Tech., 2010. © 2010 Wiley‐Liss, Inc.