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Determination of low molecular weight aliphatic amines by HPLC in environmental water samples

✍ Scribed by Djozan, Dj. ;Faraj-Zadeh, M. A.

Publisher
John Wiley and Sons
Year
1996
Tongue
English
Weight
444 KB
Volume
19
Category
Article
ISSN
0935-6304

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✦ Synopsis

Abstract

A high resolution liquid chromatographic method is described for determination of low molecular weight (LMW) aliphatic amines in environmental waters. The analytes after isolation are derivatized by fluram and separated with isocratic elution on octyl (C~8~) column, followed by fluorimetric detection in 395/495 nm. Different isolation procedures such as octadecylsilane (ODS) and strong cation exchanger (SCX) solid phase extraction (SPE) cartridges and Amberlite CG‐120 resin were evaluated. The quantitative characteristics such as recovery, linear dynamic range, correlation coefficient, limit of detection (LOD), and relative standard deviation (RSD) are presented. Using this method, aliphatic amines were analyzed in rain and tap water as well as in waste water.

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