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Determination of ethylphenols in wine by in situ derivatisation and headspace solid-phase microextraction–gas chromatography–mass spectrometry

✍ Scribed by José David Carrillo; María Teresa Tena

Publisher
Springer
Year
2007
Tongue
English
Weight
809 KB
Volume
387
Category
Article
ISSN
1618-2650

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Speciation of inorganic and tetramethylt
Speciation of inorganic and tetramethyltin by headspace solid-phase microextraction and gas chromatography–mass spectrometry
✍ Nikolaos M. Tzollas; George A. Zachariadis 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 180 KB

## Abstract A headspace solid‐phase microextraction (HS‐SPME) method coupled to GC‐MS was developed in order to determine trace levels of tetramethyltin (TeMT) and inorganic tin (iSn) after ethylation to tetraethyltin (TeET) in various matrices. The derivatization of iSn and the extraction of both