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Determination of double bond position in mono-unsaturated acetates by mass spectrometry of dimethyl disulfide adducts

โœ Scribed by Buser, Hans Rudolf.; Arn, Heinrich.; Guerin, Patrick.; Rauscher, Stefan.

Book ID
120423373
Publisher
American Chemical Society
Year
1983
Tongue
English
Weight
539 KB
Volume
55
Category
Article
ISSN
0003-2700

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Determination of double-bond positions i
Determination of double-bond positions in methylene-interrupted dienoic fatty acids by GC-MS as their dimethyl disulfide adducts
โœ Kohei Yamamoto; Akira Shibahara; Takao Nakayama; Goro Kajimoto ๐Ÿ“‚ Article ๐Ÿ“… 1991 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 771 KB

A method using GC-MS for determining the double-bond positions in methylene-interrupted dienoic fatty acids as their dimethyl disulfide adducts is described. As a standard procedure for the single-step preparation of the adducts, methyl linoleate was subjected to the 12-catalyzed reaction with dimet