The structure of AlVMoOr was solved by direct methods from high resolution X-ray powder diffraction data and refined by the Rietveld method. The lattice constants are a=5.3763(3)& b=8.1644(3)A and c=12.7312A. S pace group Pmcn followed from the systematic extinctions and was confirmed by the success
✦ LIBER ✦
Determination of crystal structures with large known fragments directly from measured X-ray powder diffraction intensities
✍ Scribed by Rius, J. ;Miravitlles, C.
- Book ID
- 114500067
- Publisher
- International Union of Crystallography
- Year
- 1988
- Tongue
- English
- Weight
- 326 KB
- Volume
- 21
- Category
- Article
- ISSN
- 0021-8898
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## Abstract The crystal structures of the dispiro compounds 1,3,4,8,10,11‐Hexaphenyl‐13‐methyl‐1,2,8,9,13‐pentaazadispiro[4.1.4.3]tetradeca‐2,9‐dien‐6‐one (**3a**) and 4,11‐Bis(4‐methoxyphenyl)‐13‐methyl‐1,3,8,10‐tetraphenyl‐1,2,8,9,13‐pentaazadispiro‐[4.1.4.3]tetradeca‐2,9‐dien‐6‐one (**3b**) have