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Determination of carbon and hydrogen by Pregl's method. A new form of heating mortar

✍ Scribed by Kirby, H.


Publisher
Wiley (John Wiley & Sons)
Year
1939
Weight
135 KB
Volume
58
Category
Article
ISSN
0368-4075

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A new method for structure determination
✍ Wolfgang Voelter; Eberhard Breitmaier; GΓΌnther Jung; Ernst Bayer πŸ“‚ Article πŸ“… 1970 πŸ› John Wiley and Sons 🌐 English βš– 168 KB πŸ‘ 1 views

## Abstract A useful method for the assignment of hydroxyl groups in steroids is described in which hydroxy‐steroids are reacted with trifluoroacetic anhydride. The δ‐values of the CF~3~ signals from the resulting trifluoroacetates characterize the positions of the trifluoroacetylated hydroxyl grou