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Determination of Boron in Borohydrides and Organoboron Compounds by Oxidation with Trifluoroperoxyacetic Acid

✍ Scribed by Strahm, R. D.; Hawthorne, M. F.

Book ID
126306822
Publisher
American Chemical Society
Year
1960
Tongue
English
Weight
297 KB
Volume
32
Category
Article
ISSN
0003-2700

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Sulphite (5.0 X lo-'-5.0 X lo-' M), ascorbic acid and other compounds are oxidized by potassium iodate in dilute sulphuric acid; the production of iodide is monitored by an iodide-selective electrode. The time needed for a 40-mV potential change is inversely proportional to concentration. For sulphi