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Determination of biogenic quaternary ammonium compounds on fused silica capillary columns with a splitless injector as a chemical reactor/pyrolysis chamber

✍ Scribed by Findeis, P. M. ;Farwell, S. O.


Publisher
John Wiley and Sons
Year
1984
Tongue
English
Weight
456 KB
Volume
7
Category
Article
ISSN
0935-6304

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✦ Synopsis


A conventional splitless injector is used as a pyrolysis chamber or chemical reactorfortheN-demethylation of acetylcholineand other choline esters. The novel uses of 2-aminoethanol as a Ndemethylation reagent in splitless injection and bonded-phase fused silica capillary columns in the separation of the tertiary amine derivatives of choline esters are described. A comparison is made between non-polar and moderately polar fused silica capillary columns in the separation of choline esters.