A simple and rapid hydride generation—at
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R.G. Smith; J.C. Van Loon; J.R. Knechtel; J.L. Fraser; A.E. Pitts; A.E. Hodges
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Article
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1977
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Elsevier Science
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English
⚖ 581 KB
An inexpensive 50-ml disposable (hypodermic) syringe is used as the arsine generation vessel. The arsine is passed into a lo-cm long. lo-mm i.d. electrically heated silica tube atomizer with nitrogen carrier gas. Jkcess of hydrogen is burned off in a hydrogen diffusion flame at the ends of the tube.