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Determination of ammonium regeneration rates in the oligotrophic ocean by gas chromatography/mass spectrometry

✍ Scribed by Darren R. Clark; Tim W. Fileman; Ian Joint


Publisher
Elsevier Science
Year
2006
Tongue
English
Weight
167 KB
Volume
98
Category
Article
ISSN
0304-4203

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A method for determining the rate of exchange of the carbonyl oxygen in ~-ketoglutarate using gas chromatography-mass spectrometry is described. The method is based on a new procedure for quenching the exchange reaction by rapid oxidative decarboxylation of the LYketoacid to the next lower homologou