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Determination of a molecular crystal structure by X-ray powder diffraction on a conventional laboratory instrument

✍ Scribed by Lightfoot, Philip; Tremayne, Maryjane; Harris, Kenneth D. M.; Bruce, Peter G.

Book ID
118002938
Publisher
The Royal Society of Chemistry
Year
1992
Tongue
English
Weight
305 KB
Volume
14
Category
Article
ISSN
0022-4936

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## Abstract The crystal structures of the dispiro compounds 1,3,4,8,10,11‐Hexaphenyl‐13‐methyl‐1,2,8,9,13‐pentaazadispiro[4.1.4.3]tetradeca‐2,9‐dien‐6‐one (**3a**) and 4,11‐Bis(4‐methoxyphenyl)‐13‐methyl‐1,3,8,10‐tetraphenyl‐1,2,8,9,13‐pentaazadispiro‐[4.1.4.3]tetradeca‐2,9‐dien‐6‐one (**3b**) have