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Derivate natürlicher Tetrapyrrole für die Photodynamische Therapie, 2 Modellreaktionen zur direkten CC-Verknüpfung von Porphyrinen

✍ Scribed by Risch, Nikolaus ;Mackenbrock, Ursula


Publisher
John Wiley and Sons
Year
1992
Tongue
English
Weight
434 KB
Volume
1992
Category
Article
ISSN
0947-3440

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✦ Synopsis


Natural Tetrapyrrol Derivatives for the Photodynamic Therapy, 2. — Model Reactions for Direct C–C Linkages of Porphyrins

Until now, there is a lack of information about the structure of the active components in the diagnosis and photodynamic therapy of cancer with hematoporphyrin derivatives (HPD). We describe the formation of HPD in terms of benzyl cation chemistry. Selective formation of the C—C‐linked model compounds 4, 5 by reaction of protoporphyrin dimethyl ester (2) with electron‐rich aromatic compounds as well as of 9—12, 15–17, obtained by reaction of the porphyrin dimethyl esters 2, 6, 7, and 8, with carbon electrophiles (preformed Mannich salts), results from this concept.