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Demonstration of Isomers and Intramolecular Isomerization of Carbene Complexes of Chromium

✍ Scribed by Prof. Dr. Ernst Otto Fischer; Dipl.-Chem. Helmut Fischer; Prof. Dr. Helmut Werner

Publisher
John Wiley and Sons
Year
1972
Tongue
English
Weight
213 KB
Volume
11
Category
Article
ISSN
0044-8249

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Treatment of (CO) 5 W=C(NMe 2 )CH=CH-Ar-(OH)(H)CϵCH (1a-b) [a: -Ar-=1,4-C 6 H 4 -; b: -Ar-= 2,5-C 4 H 2 S-] with W(CO) 5 (THF) in methanol yields the nonsymmetrical bis(alkenylcarbene)-bridged ditungsten complexes (CO) 5 W= C(NMe 2 )CH=CH-Ar-CH=CH(OMe)C=W(CO) 5 (3a-b). Similarly, the symmetrical bis